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Smaller tank = easier?

Mike, pH is not concentration, so you can't calculate that way. It's the negative log of the hydrogen ion concentration.

Here's useful info from the Randy article:

4. Delivering a small amount of limewater all at once. Adding 1.25% of the aquarium’s volume (1.25 gallons of limewater per 100 gallons of aquarium water) as saturated limewater all at once raises the pH by 0.6 to 0.7 pH units. Such an increase is clearly too large. Adding a smaller portion all at once can, however, be acceptable. Adding, for example, 0.25% of the aquarium volume (0.25 gallons or 1 L of limewater per 100 gallons of aquarium water) will raise the pH by only 0.1 to 0.2 pH units. Unless the pH is high (>8.4) before the addition, that amount is likely acceptable. The other concern with all-at-once dosing is that the local pH in the area of the addition will rise considerably higher than the values above. So dosing must be done far from living organisms, and in high flow areas that will facilitate fast mixture. In some aquaria, such restrictions make all-at-once dosing of limewater prohibitively risky to living organisms.

1 gallon of saturated kalk water would give you a .4 meq rise in alk. Too much at once for that method.
 
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